If you choose to powder the root bark the waterless de-fat method without the need for acid uses only solvent alone for a defat and has proven to work well with any kind of powdered alkaloid bearing root bark.
easy to do with 2 hoses (e.g. . Although the initial yield will be much higher if extracting powdered root bark which takes much less time, whole or broken root bark can also provide high yields if you wait two or three days for the hard strips of bark to turn into a mush as the NaOH breaks it down further and further over time in the basified solution for a higher extraction yield. This is what I have been doing and have gotten between 770mg-1.1g of spice. I don't know if this will be of much benefit because I've never done this myself but for an extreme defat heat your can of naphtha in some hot tap water coming out of your facet at a temperature of at least 100 degree F., once the solvent is hot then stir the powder into it but be sure to pour off and strain every drop of naphtha you can when done and later throw that naphtha away, you should not use this naphtha for anything more in the process. An updated and edited reprint of the same-named article from The Entheogen Review, Autumnal Equinox 2006, Volume XV, Number 3, edited by noman and zhah March, 2007. If you decide to heat your basified mix with naphtha in it for hours to days as the root bark is broken down by the NaOH I would cover the container with kitchen plastic wrap or something to slow the evaporation of the naphtha. That's it, a very simple process with yields others have reported to be much higher than the more often used A-B or acid to base teks. And don’t forget to scrub those jars and utensils with your favorite smoking herb!
Decant naptha into evap dish. If waiting 24 hours and performing a single extraction the broken root bark the basified aqueous mix will still need to be extracted over again three or more times to get more of the alkaloid out. Materials. swims cat just mixed 100g's powdered MHRB into his basified solution of water+100g's of NaOH and has stirred/mixed and put it away for a an hour or so.
An hour before pouring it off the mix was warmed to 120° F. and stirred for 20 minutes. . Minimize airflow above your final evaporation dish, [e.g. So, try it either way but don't give up too soon, see for yourself if you have more goodies to get by soaking the plant material longer, even if powdered. Anecdotal reports say that MHRB (standardly rated at 0.57% DMT) can provide from 1-2% DMT if a zinc powder reduction is used beforehand. While I have not verified this report I did get a runny extra Airflow turns DMT into DMT-oxide, which is yellow, sticky and apparently not as strong (or different effect) depending on who you talk to. No need to powder the root bark, just break into small pieces and extract whole, no need for the use of a separation funnel or baggies modified to act as one. swims cat wanted me to post this here in case he runs into any problems and also just to document the progress of his extraction.
. Note: When the solvent was evaporated from the defat process there was no discernible amount of alkaloid present, only orange fats.
A- use a separatory funnel if you can get one, or - The short story about this tek: This was the first MHRB tek on the net for extracting the desired alkaloid from MHRB using broken or solid pieces of root bark without the need to powder the material but is actually a better process for powdered. E - Suck up with a hose using your lungs... like siphoning petrol, , it'll work, but probably hurt your brain long term. Extraction yields from one pound of inner MHRB: First extraction cycle: 1 gram in 2.5 hrs.
Take off top from the bottle, expel air, replace cap. The intent of this tek is to simplify the extraction procedure as much as possible and make it doable for the average person in the average kitchen in an evening. If you want to make DMT oxide add Hydrogen Peroxide (H2O2) to your DMT later.
To assure this substance does not extract along with the alkaloid it might be better to just leave the solution at normal room temperatures while soaking the bark in the aqueous mix for 72+ hours and only raise the solution to 120° F. for an hour prior to pouring the solvent off for evaporation. Although recrystallization inevitably results in loss of goods, once you’ve had a hit of DMT that left absolutely NOTHING behind in the pipe, you won’t want to use anything else.
When soaking the root bark in the warmed solution be sure to periodically check the temperature to make sure the solution does not go over 120° F. or you might get a lot of the gummy impurities in the extract which showed up when I did so. This will make the freeze precipitation better.
B - Don't blow a fan over your white crystals, they will go yellow and start absorbing water and go gooey. The solvent will be a clear yellow. peace tenstrip SWIM used 50g of root bark to 750ml of water and 75g of NaOH, SWIM then used .6ml of naphtha per gram of bark (.4ml did not give enough depth to the separation layer in the size jar SWIM was using) 7 pulls of 30ml (first pull 20ml) yielded the following pure white precipitation; 1)101mg 2)107mg 3)72mg 4)41mg 5)23mg 6)8mg 7)8mg and 40mg off the shot glasses used for the freeze precipitation for a total of 400mg, all pulls were with room temp naphtha. You should read a few teks before deciding on one and research the chemicals and procedures that you will be using. How long should you defat in naptha?
total weight from fuel extraction off of entire mixture. You should treat this procedure as a starting point from which it is up to you to discover the best way to proceed based upon the materials and equipment available to you.
if that. Perhaps heating the mix allows plant fats to come over which did not do so before?
It tends to get contaminated with other plant oils etc that reduce the amount of DMT that can enter the solution. Base Material: 1 lb Powdered or finely ground MHRB (Mimosa Tenuiflora/Hostilis root bark). 50g MHRB DMT Extraction Tek This is basically cybs max ion tek, with the slight alterations of adding more vinegar, salt and slightly more lye.